Lifting and rotating double jacketed glass reactor:

The inner container of the chemglass 20l jacketed reactor kettle can be lifted and rotated to place the reaction materials, and at the same time, it can be vacuumized and stirred at a speed. It is used for experiment, pilot test and production in chemistry, fine chemical industry, biopharmaceutical new material synthesis, etc. The product can be combined with circulating water-type multi-purpose vacuum pump, diaphragm vacuum pump, low temperature circulating (vacuum) pump, circulating cooler, constant temperature circulator, low temperature cooling liquid circulating pump, closed refrigeration heating circulating device, etc. to form a 50l jacketed glass reactor system device.

Lifting and rotating double-layer glass reactor features:

1. The kettle body can be raised and lowered manually, which is convenient for feeding and taking out bulk crystals. It can be rotated 0~120° for easy cleaning.
2. New design, stable body during operation.
3. The sealing method of flange connection is adopted, no vacuum grease sealing, good sealing performance and high vacuum degree.
4. The bottom discharge design without dead angle makes the medicine in the kettle fully mix and react, which is convenient for cleaning and prevents cross-contamination between medicines.
 

The complete system usually includes:

1 The main body of the laboratory glass reactor
2 stirring unit
3 Vacuum unit
4 Temperature control unit
5 Liquid feeding and liquid dripping unit
6 Kettle lifting and rotating unit
7 Other special customized units (sand filter system)
 

Detailed description of main components:

1. laboratory glass reactor part: single-layer, double-layer, three-layer
Jacketed reactor, high borosilicate glass (3.3) material Working volume: 5L 10L 20L 30L 50L Split type lower discharge valve opening , liquid feeding, etc. The kettle cover and the kettle body are connected by handwheel lifting and extrusion type sealing. All parts in contact with the liquid are made of borosilicate glass or PTFE material, and some are designed with parallel steel bases to resist chemical corrosion, and the body is stable under running conditions. , and is equipped with casters for easy movement. The whole system can be moved at the same time to ensure the stability of the whole set of equipment and the flexibility of space placement
 
2. Stirring part
The top-mounted stirring system ensures the stability of the whole set of equipment. The double-sealed stirring and sealing bearings ensure the high sealing performance of the glass reactor supplier system. Glass, stainless steel and PTFE-coated fluorine materials can be selected. Easy to replace other forms of stirring paste
 
3. Vacuum unit
Various models of vacuum/pressure pumps are available for selection. Diaphragm Vacuum Pump Rotary Vane Oil Sealed Vacuum Pump Circulating Water Type Multipurpose Vacuum Pump
4. Temperature control part
Digital display stirring speed, frequency conversion, constant speed stirring system, stable operation, optional explosion-proof control system
 

Working principle of laboratory glass reactor:

Distillation, many people know this term, but it is really specific to the principle of distillation and how it is carried out. I believe many people are not clear. Today, I will bring you some explanations about the distillation principle of laboratory glass reactor. .
The analysis was carried out by taking the separation of two-component mixture as an example. After the raw material liquid is heated, partial vaporization will occur, in which the volatile components will be concentrated in the steam, while the remaining liquid will produce higher non-volatile components, which achieves the separation of the two to a certain extent. . The greater the difference in volatilization between the two, the greater the concentration of the two substances. Using an industrial rectification device, the partially evaporated liquid phase is directly contacted with the partially condensed gas phase, thereby realizing partial evaporation of the liquid phase and partial condensation of the gas phase, that is, partial evaporation of the gas phase and partial condensation of the gas phase, so as to realize the partial evaporation of the gas phase and the partial condensation of the gas phase. Partial evaporation and partial condensation of the gas phase.
 
The molecules of the liquid tend to spill over the surface due to molecular motion. This trend increases with increasing temperature. When a liquid is placed in a closed vacuum system, the molecules of the liquid will continuously escape, forming a vapor on the surface of the liquid, after which the molecules will escape from the vapor, and then the molecules will escape from the vapor back into the liquid, and the vapor remains certain pressure. At this point in time, the liquid surface is saturated, which is called saturated vapor, and the pressure it exerts on the liquid surface is called the saturated vapor pressure. The results show that the saturated vapor pressure of the liquid is only related to the temperature, that is, the liquid has a certain vapor pressure at a certain temperature. Refers to the pressure under which a liquid is in equilibrium with its vapor, regardless of the amount of liquid and vapor in the system.
 
The combined operation of heating a liquid until it boils, turning it into a vapor, and then cooling the vapor and condensing it into a liquid is called distillation. Obviously, distillation can separate volatile and non-volatile substances, as well as mixed liquids with different boiling points. However, in order to obtain a good separation effect, the boiling points of each component of the mixture must be very different (at least 30°C or more). During atmospheric distillation, since the atmospheric pressure is usually not exactly 0.1MPa, strictly speaking, the boiling point plus the correction value should be observed, but since the deviation is usually small, even if the atmospheric pressure differs from the atmospheric pressure by 2.7KPa, the correction value is only ± 1°C, so it can be ignored.

 

Parameter:

Model: GRL-10L 20L 30L 50L 80L 100L 150L
Material of kettle body: high borosilicate glass
Temperature sensor material: stainless steel covered with PTFE, double anti-corrosion
Working temperature (℃): -80～200℃
Adjustment method: frequency conversion speed regulation
Can withstand the temperature difference between inside and outside the jacket: 60°C (three layers), 110°C (two layers)
Inlet and outflow circulation port: Buffer tube at the circulation port of the kettle body to protect the kettle body
Power (V/Hz): 220V~240V, 50/60Hz
 
The above is what ZZKD Co., Ltd. brings to you about the distillation principle of thelaboratory glass reactor. If you have any questions, you can contact us at any time, and we will serve you wholeheartedly.
ZZKD Co., Ltd. provides you with glass reactors of various specifications and models, and supports customization.