Double layer stirred glass reactor manufacturer | ZZKD
What is a double-glass reactor?
The double-layer glass reactor is designed as double-layer glass, and the inner layer is placed in the reaction medium for stirring reaction, and the interlayer can be heated or cooled by using different cold and heat sources (refrigerant, hot water or hot oil). Under the constant temperature condition, in a closed glass reactor, the stirring reaction can be carried out under normal pressure or negative pressure according to the use requirements, and the reflux and distillation of the reaction solution can be performed. It is a modern fine chemical factory, biopharmaceutical and The ideal pilot and production equipment for the synthesis of new materials.
Glass reactors produced by glass reactor manufacturer ZZKD have capacities of 1 L, 2 L, 3 L, 5 L, 10 L, 20 L, 30 L, 50 L, 100 L.
Glass reactors produced by glass reactor manufacturer ZZKD have capacities of 1 L, 2 L, 3 L, 5 L, 10 L, 20 L, 30 L, 50 L, 100 L.
| Model | S-50L Jacketed Glass Reactor |
|---|---|
| Stirring Power(W) | 120 |
| Stirring Speed(rpm) | 0~600(max.1300) |
| Stirring Shaft Diameter(mm) | 12 |
| Reaction Flask Capacity(L) | 50 |
| Voltage(V/Hz) | 220 50/60 |
| Motor Torque(g/cm) | 1500 |
| Note | 304 All Stainless Steel Frame |
How the double-layer glass reactor works
The double-layer glass reactor interlayer is injected with a constant temperature (high temperature or low temperature) hot-dissolving medium or a cooling medium, and the contents of the reactor are heated or cooled at a constant temperature, and stirring can be provided. The material is reacted in the reaction kettle, and the evaporation and reflux of the reaction solution can be controlled. After the reaction is completed, the material can be discharged from the discharge port of the bottom of the kettle, and the operation is extremely convenient. It is an ideal equipment for modern chemical samples, sample experiments, biopharmaceuticals and new materials. Can provide high temperature reaction (configure the corresponding circulating oil bath, the maximum temperature can reach 300 ° C); can also do low temperature reaction (configure the corresponding low temperature chilling liquid circulation system, the lowest temperature can reach -80 ° C); Vacuum to do the vacuum reaction. Moreover, its unique design makes the test safer and more convenient.
Main feature
1. Frequency control, AC induction motor. Constant speed, no brush, no spark, safe and stable, can work continuously.
2. The complete glass instrument is made of GG17 borosilicate glass and has good chemical and physical properties.
3. The glass interlayer interface is connected to the hot oil through the circulation, which can be used for heating reaction, and the low temperature reaction can be carried out by using the frozen liquid.
4. It can react at room temperature, and it can quickly take away the reflected heat when it is connected to tap water.
5. The lower discharge port has a flange mouth and a polytetrafluoroethylene valve. There is no dead angle in the container, and it can be disassembled to facilitate the discharge of solid materials.
6. Four-port reactor cover, the special port design is easy to clean, and the standard port socket can be assembled and reflowed, and the distillation synthesis device.
Instructions for use
1. Please familiarize yourself with the contents of this manual before installation, use, maintenance and inspection.
2. The power supply voltage must be the same as specified in the instrument.
3. No load is not suitable for high speed operation.
4. The life of the electrical box and the surrounding temperature, the impact of humidity is great. Please keep the speed and the motor dry.
5. Install the machine first and then be wired by a professional electrician. The ground terminal must be grounded. The high temperature bath must be connected to the open switch.
6. Within 5 minutes after the power is turned off, there is a possibility of electric shock due to discharge of the inverter or capacitor.
7. Pay attention to the impact damage of the hard object (watch, ring, belt buckle, etc.) on the glass during the operation.
8. Be careful when connecting the vacuum tube or water pipe to avoid excessive damage to the human body caused by the glass.
9. When using high-temperature circulating oil bath, pay attention to the damage of high temperature to the human body. It is recommended to use a heat-conducting oil (dimethicone, kinematic viscosity of 100) which is harmful to human body as a solvent. In particular, when paying attention to high temperature circulation, the circulating pump should be turned on first to allow the heat transfer solvent to circulate, and then slowly heat up.
Instrument installation
1. After opening the package, check whether the main accessories of the machine are complete according to the packing list.
2. Assemble the frame according to the drawing of the stainless steel tube and the fixing piece.
3. Install the electrical box on the top of the right rear pole and tighten the screws and insert the seven-pin plug. Install the vacuum gauge on the left rear end and tighten the screws.
4. According to the height of use, fix the round bracket of the kettle to the vertical pole slider, and place the kettle on the bracket. The semi-circular hoop is used to insert the pole of the kettle into the pole of the kettle, and then tighten the fixing screws after closing. Pay attention to the vertical direction of the reactor body during installation.
5. The stir bar is fixed on the toothed ring chuck of the motor main shaft. The stir bar passes through the middle rotating bearing of the cover, tightens the special connector, and then adjusts the position of the motor, paying attention to the vertical concentricity.
6. The slider on the pole is a stainless steel multi-purpose clamp that adjusts the direction and height in different directions.
7. On the left side of the bottle cap, the 40# standard port plug-in type reflux condenser, the right side 40# is the feeding port connected to the constant pressure funnel, the middle front 24# standard port is inserted into the thermometer casing mouth, and the rear of the hat is the 34# standard port. It is a multi-functional spare port, and the bottom is provided with a discharge valve, and the bottom of the kettle body is respectively a circulating fluid inlet and outlet. The lower port is connected to the circulating fluid inlet, and the upper port is connected to the circulating fluid return port.
8. When installing the glass instrument, it must be cleaned, and the interface should be coated with Vaseline to prevent the glass from locking up, and then apply vacuum grease to prevent air leakage.
9. Press the universal wheel wheel fixing device to stir. If the stirring is stable, the debugging is good.
Instructions
1. Check that the power supply voltage is consistent with the specifications provided on the machine nameplate.
2. Plug in the power plug, turn on the power switch on the inverter, and use the speed knob to select the appropriate speed.
3. The flow of material and the power of the motor speed may resonate at a certain point. Please change the speed of the motor to avoid resonance.
4. After the stir bar is installed, it must be rotated by hand. Pay attention to whether the concentricity is good. If the heart is not good, the heavy clamp should be loosened. After the clamp is turned on, turn on the power again. Adjust slowly from slow to fast. 5. Adjust with a stir bar. The stirring leaves can be up and down 5 cm as needed.
6. If the seal performance of the kettle is found to be degraded, please check the rotary bearing in the stirrer sleeve.
7. The glass equipment of this reaction device is all made of GG.17 low expansion coefficient high temperature resistant borosilicate glass. The user should self-fit glass bottles such as reaction bottles. Please confirm the quasi-glass material to ensure safe use.
8. The external layer of the interlayer on the glass kettle can be heated by the hot oil. The coolant can be used for low temperature reaction. If it is heated by steam, it should not exceed 0.5K-1K (try not to use pressure steam to heat).
9. When the test is carried out at low temperature, the discharge valve at the bottom will be frosted. When using the valve, it must be partially thawed to prevent the glass from being broken.
10. If there are particulate objects in the solution during use, it is possible to store the remaining materials on the PTFE piston of the valve. When used again, the airtightness will be affected. Be sure to clean and re-use each time after discharging. .
Maintenance instructions
1. Check the instrument carefully before use. Whether the glass bottle is damaged or not, and whether the interfaces are consistent, pay attention to light handling.
2. Wipe each interface with a soft cloth (can be replaced with a napkin) and apply a small amount of vacuum grease. (The vacuum grease must be covered after use to prevent the entry of sand.)
3, each interface can not be screwed too tight, you should loosely loosen the active, to avoid long-term tight lock caused by the connector to die.
4. Turn on the power switch first, then let the machine run from slow to fast. When the machine is stopped, stop the machine and turn off the switch.
5, the PTFE switch everywhere can not be tightened too much, easy to damage the glass.
6. Every time you use it, you must wipe off all kinds of oil stains, stains and solvents left on the surface of the machine with a soft cloth and keep it clean.
7. Loosen the PTFE switches after stopping, and the PTFE piston will be deformed when it is still working for a long time.
8. Regularly clean the sealing ring by removing the sealing ring and checking if there is dirt on the shaft. Wipe it with a soft cloth, then apply a little vacuum grease and reinstall it to keep the shaft and seal ring smooth.
9, the electrical part must not enter the water, it is strictly prohibited to get wet.
10, must purchase the original authentic accessories, free use of other accessories can cause fatal damage to the machine.
11. When doing any repairs or inspections on the machine, be sure to cut off the power supply and water source. Note that this equipment is a fragile product, please be careful when using it. The damage of fragile goods is not covered by our warranty. If the customer needs, we will charge the corresponding cost.
Troubleshooting editor
1. Turn on the power switch and the indicator light does not light. The external power supply is not connected or the contact is poor. Please check the power supply and socket with a professional electrician.
2. Short-circuit the fuse. Set the power switch to the OFF position and replace the fuse.
3. The power indicator is on but not rotating. Rusting of the rotating shaft Stop using and contact the supplier Motor, electrical box failure The seven-pin plug is not connected, reconnect the seven-pin plug.
4. The vacuum suddenly disappears, the glass has cracks, the switch is damaged, check the glass parts, and change the switch.
5. There is vacuum, but it can't be pumped. The seal ring is worn and the vacuum switch is connected. Please replace the seal ring and switch.
6. Sometimes there is no vacuum. There are loose connectors on the steel shaft. Please remove the dirt and check the vacuum gauge and vacuum pump.
7. The vacuum hose is aging, please replace the vacuum hose.
8. The main mandrel is loose left and right, and the tight top screw is loose and tightened.
10, the motor temperature is too high (room temperature plus 40 ° C is normal), overload, stop, hand-turn the machine shaft, whether it is very heavy, remove the dirt on the contact between the seal ring and the glass shaft, apply vacuum grease.
11. The speed display does not match the actual one. The voltage is unstable and there is error in itself. Contact the supplier.
12, the outer casing is charged, the heating pipe has cracks into the water, please check with a professional electrician.