Cylindrical jacketed glass reactor maintenance
Technical Maintenance Method - Double Layer Glass Reactor Technical Features Description:
1. The whole stainless steel column mobile frame structure, five reactor covers, complete glass with reflux, liquid addition, and temperature measurement.
2. G3.3 borosilicate glass is used, which has good chemical and physical properties.
3. alloy steel mechanical seal, Teflon joint, to maintain high-precision sealing under working conditions.
4. Pt100 sensor probe, high-temperature measurement accuracy, a small error, effectively improves work efficiency.
5. Germany technical exchange gear reduction motor, strong torque, no noise.
6. double PTFE stirring paddle, suitable for mixing and mixing of low to high viscosity liquid.
7. PTFE discharge valve, movable interface, the discharge is completely fast.
The jacketed glass reactor vessel is designed as a double-layer glass. The working principle is that a reaction solvent can be placed in the inner layer of the glass to perform a stirring reaction, and the interlayer can be made by diverging cold heat sources (refrigerant, hot water or hot oil). Circulating heating or cooling the reaction. Through the process, a cylindrical reactor interlayer, a constant temperature (low temperature or low temperature) hot-dissolving medium or cooling medium is injected to uniformly heat or cool the materials in the reactor. At the same time, the stirring reaction can be carried out under normal or negative pressure conditions in accordance with the operation request. The material is reacted in the reactor, and the evaporation and reflux of the reaction solution can be controlled. After the reaction is finished, the material can be discharged from the discharge port of the bottom of the vessel.
Borosilicate glass reactor maintenance instructions:
1. Check the instrument carefully before use. Whether the glass bottle is damaged or not, and whether the interfaces are consistent, pay attention to light handling.
2. Wipe each interface with a soft cloth (can be replaced with a napkin) and apply a small amount of vacuum grease. (The vacuum grease must be covered after use to prevent the entry of sand.)
3. each interface can not be screwed too tight, you should loosely loosen the active, to avoid long-term tight lock caused by the connector to die.
4. Turn on the power switch first, then let the machine run from slow to fast. When the machine is stopped, stop the machine and turn off the switch.
5. the PTFE switch everywhere can not be tightened too much, easy to damage the glass.
6. Every time you use it, you must wipe off all kinds of oil stains, stains and solvents left on the surface of the machine with a soft cloth and keep it clean.
7. Loosen the PTFE switches after stopping, and the PTFE piston will be deformed when it is still working for a long time.
8. Regularly clean the sealing ring by removing the sealing ring and checking if there is dirt on the shaft. Wipe it with a soft cloth, then apply a little vacuum grease and reinstall it to keep the shaft and seal ring smooth.
9. the electrical part must not enter the water, it is strictly prohibited to get wet.