Installation:

 

1. Open the packing case, and check all components. 

 

2. Bring out the stainless steel frame, adjust the support ring to a suitable position.

 

3. Mount the jacketed flask on the stainless steel frame. Adjust the support ring and tighten the screws.

 

4. Install the main rod, condenser support and all connecting rods.

 

5. Install the motor and frequency converter.

 

6. Install the stirring sealing components to the glass cap. Insert the stirring rod and close the cap. Coating a little bit grease on the sealing surface can reduce wear and tear of glassware and ensure a high vacuum degree.

 

7. Install all the glass components and coat sealing surface with silicon grease.

 

8. Mount the discharge valve on the bottom of jacketed flask.

 

9. Check all the installation steps, when all the adjustments are done, you can power on to test the device.

Double-layer-glass-reactor-structure-diagram

 

Operation procedures:

 

1. Check the supply voltage to ensure it is consistent with the specifications of the device.

 

2. Connect plug to power socket, turn on the frequency converter, rotate the rotation knob to set suitable rotation speed.

 

3. After installing the stirring rod, rotate it by hand to check if the concentricity is good. If not，adjust it gradually from slow to fast.

 

4. If the sealing performance become weaker, please check the the rotating bearing seal in the stirrer.

 

5. Adopt GG17 high-borosilicate glass with nice physical-chemical properties.

 

6. Move mixing blades up and down 5cm according to the actual need.  

 

7. Circulation port on the outside of interlayers, can do heating reaction using hot oil, do low temperature reaction using coolant. If use steam heat, not more than 0.5 K - 1K (Better not to use pressure steam heating).   

 

8. The discharge valve at the bottom will be frosted under low temperature environment, please thaw before using the valve in case of breaking the glass.

 

9. If there are particles in reaction solution, please wash valve carefully after draining because the particles remaining in the valve will affect the tightness.